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Ultrasound Modulates Calcium Activity in Cultured Neurons, Glial Cells, Endothelial Cells and Pericytes

Malachy Newman, Pratheepa Kumari Rasiah, Jiro Kusunose, Tonia S. Rex, Anita Mahadevan-Jansen, Jacob Hardenburger, E. Duco Jansen, Bryan Millis, Charles F. Caskey

Ultrasound in Medicine & Biology 2024, 50, 341-351 · 10.1016/j.ultrasmedbio.2023.11.004

in vitro cellhealthycellular imaginghistology molecular

Abstract

Objective Ultrasound is being researched as a method to modulate the brain. Studies of the interaction of sound with neurons support the hypothesis that mechanosensitive ion channels play an important role in ultrasound neuromodulation. The response of cells other than neurons (e.g., astrocytes, pericytes and endothelial cells) have not been fully characterized, despite playing an important role in brain function. Methods To address this gap in knowledge, we examined cultured murine primary cortical neurons, astrocytes, endothelial cells and pericytes in an in vitro widefield microscopy setup during application of a 500 ms burst of 250 kHz focused ultrasound over a pressure range known to elicit neuromodulation. We examined cell membrane health in response to a range of pulses and used optical calcium indicators in conjunction with pharmacological antagonists to selectively block different groups of thermo- and mechanosensitive ion channels known to be responsive to ultrasound. Results All cell types experienced an increase in calcium fluorescence in response to ultrasound. Gadolinium (Gad), 2-aminoethoxydiphenyl borate (2-APB) and ruthenium red (RR) reduced the percentage of responding neurons and magnitude of response. The percentage of astrocytes responding was significantly lowered only by Gad, whereas both 2-APB and Gad decreased the amplitude of the fluorescence response. 2-APB decreased the percentage of responding endothelial cells, whereas only Gad reduced the magnitude of responses. Pericytes exposed to RR or Gad were less likely to respond to stimulation. RR had no detectable effect on the magnitude of the pericyte responses while 2-APB and Gad significantly decreased the fluorescence intensity, despite not affecting the percentage responding. Conclusion Our study highlights the role of non-neuronal cells during FUS neuromodulation. All of the investigated cell types are sensitive to mechanical ultrasound stimulation and rely on mechanosensitive ion channels to undergo ultrasound neuromodulation.

Abstract via europepmc.

SpeciesSprague-Dawley rat (primary cortical neurons and astrocytes); human (primary pericytes and brain cortex microvascular endothelial cells)
Subjectsnot reported cultures
Sessions per subjectnot applicable
Randomisednot applicable
Blindingnot applicable
Sham / controlundescribed
Auditory controlnot reported
Readout timingboth
Anaesthesianot applicable
Readoutscellular imaging, histology molecularWidefield calcium fluorescence imaging (Calbryte 520); caspase-3/7 apoptosis assay; membrane integrity (MemBrite) and dye-inclusion (10 kDa dextran) assay
Direction of effectexcitatoryAll examined cell types (neurons, astrocytes, endothelial cells, pericytes) showed increased calcium fluorescence (activation) in response to ultrasound, reduced to varying degrees by mechanosensitive/TRP channel antagonists (gadolinium, 2-APB, ruthenium red) and calcium-free medium.
Adverse eventsobservedApoptosis (caspase-3/7) and membrane deformation increased with pressure in neurons and astrocytes (e.g., dye-inclusion showed 13.3% of astrocytes and 24.4% of neurons porated after exposure), but at 450 kPa no significant increase in apoptosis or membrane/cell-death markers was observed in endothelial cells or pericytes.

Exposures

Exposure 1: Primary rat cortical neurons, dosimetric pressure sweep

Target: cultured neurons — “Primary rat cortical neurons
Device: Sonic Concepts · Sonic Concepts · H115

Pulse timing
Waveformcontinuous
Fundamental frequency (kHz)250✓✓
Pulse duration (ms)not applicable
Pulse repetition frequency (Hz)not applicable
Duty cycle (%)100✓✓
Sonication duration (s)0.5✓✓
Pressure and intensity, by domain
Free-field pressure (kPa)not reported
Free-field Isppa (W/cm²)not reported
Free-field Ispta (W/cm²)not reported
In-situ estimatenot applicable
In-situ pressure (kPa)not applicable
In-situ Isppa (W/cm²)not applicable
In-situ Ispta (W/cm²)not applicable
Pressure, domain unspecified (kPa)450, 900, 1,350swept✓✓
Protocol, in the paper’s words

Cells were exposed to a single 500 ms burst with a 100% duty cycle. Exposures consisted of a single pulse with 125,000 cycles at 250 kHz.

Exposure 2: Primary rat cortical astrocytes, dosimetric pressure sweep

Target: cultured glia — “Primary rat cortical astrocytes
Device: Sonic Concepts · Sonic Concepts · H115

Pulse timing
Waveformcontinuous
Fundamental frequency (kHz)250✓✓
Pulse duration (ms)not applicable
Pulse repetition frequency (Hz)not applicable
Duty cycle (%)100✓✓
Sonication duration (s)0.5✓✓
Pressure and intensity, by domain
Free-field pressure (kPa)not reported
Free-field Isppa (W/cm²)not reported
Free-field Ispta (W/cm²)not reported
In-situ estimatenot applicable
In-situ pressure (kPa)not applicable
In-situ Isppa (W/cm²)not applicable
In-situ Ispta (W/cm²)not applicable
Pressure, domain unspecified (kPa)450, 900, 1,350swept✓✓
Protocol, in the paper’s words

Cells were exposed to a single 500 ms burst with a 100% duty cycle. Exposures consisted of a single pulse with 125,000 cycles at 250 kHz.

Exposure 3: Human brain cortex microvascular endothelial cells

Target: other — “Primary human brain cortex microvascular endothelial cells
Device: Sonic Concepts · Sonic Concepts · H115

Pulse timing
Waveformcontinuous
Fundamental frequency (kHz)250✓✓
Pulse duration (ms)not applicable
Pulse repetition frequency (Hz)not applicable
Duty cycle (%)100✓✓
Sonication duration (s)0.5✓✓
Pressure and intensity, by domain
Free-field pressure (kPa)not reported
Free-field Isppa (W/cm²)not reported
Free-field Ispta (W/cm²)not reported
In-situ estimatenot applicable
In-situ pressure (kPa)not applicable
In-situ Isppa (W/cm²)not applicable
In-situ Ispta (W/cm²)not applicable
Pressure, domain unspecified (kPa)450✓✓
Protocol, in the paper’s words

Cells were exposed to a single 500 ms burst with a 100% duty cycle. Exposures consisted of a single pulse with 125,000 cycles at 250 kHz.

Exposure 4: Human pericytes

Target: other — “Primary human pericytes
Device: Sonic Concepts · Sonic Concepts · H115

Pulse timing
Waveformcontinuous
Fundamental frequency (kHz)250✓✓
Pulse duration (ms)not applicable
Pulse repetition frequency (Hz)not applicable
Duty cycle (%)100✓✓
Sonication duration (s)0.5✓✓
Pressure and intensity, by domain
Free-field pressure (kPa)not reported
Free-field Isppa (W/cm²)not reported
Free-field Ispta (W/cm²)not reported
In-situ estimatenot applicable
In-situ pressure (kPa)not applicable
In-situ Isppa (W/cm²)not applicable
In-situ Ispta (W/cm²)not applicable
Pressure, domain unspecified (kPa)450✓✓
Protocol, in the paper’s words

Cells were exposed to a single 500 ms burst with a 100% duty cycle. Exposures consisted of a single pulse with 125,000 cycles at 250 kHz.

Flags from extraction

  • exposures[*].in_situ.pressure_kpaPaper describes both free-field (open water) and in-situ (fiber-optic hydrophone in the dish, 1 mm above cells) pressure calibration, but does not explicitly state which calibration domain the reported 0.45/0.9/1.35 MPa exposure values correspond to; assigned to in_situ because the fiber-optic hydrophone was 'selected for in situ measurements' of pressure 'within the dish' where the cells sit.
  • n_subjectsPaper reports cell counts per group (e.g., N > 200 to N > 5000 cells) but never the number of independent cultures/dishes/biological replicates used.
  • exposures[2].target.termsEndothelial cells have no matching target id in the controlled vocabulary; classified as 'other'.
  • exposures[3].target.termsPericytes have no matching target id in the controlled vocabulary; classified as 'other'.
  • sham_typePaper refers to 'sham exposures' / 'sham-exposed' cells (e.g., for endothelial cells and pericytes) without describing the sham mechanism (e.g., transducer off vs blocked); classified as 'other'.